12th INTERNATIONAL CERAMICS CONGRESS Proceedings of the 12 - download pdf or read online

By Edited by Pietro VINCENZINI World Academy of Ceramics and National Research Council, Italy Co-edited by Ralf RIEDEL Technical University of Darmstadt, Germany Alexander G. MERZHANOV ISMAN, Russia Chang-Chun

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By Edited by Pietro VINCENZINI World Academy of Ceramics and National Research Council, Italy Co-edited by Ralf RIEDEL Technical University of Darmstadt, Germany Alexander G. MERZHANOV ISMAN, Russia Chang-Chun

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Read or Download 12th INTERNATIONAL CERAMICS CONGRESS Proceedings of the 12 th International Ceramics Congress, part of CIMTEC 2010- 12 th International Ceramics Congress and 5th Forum on New Materials Montecatini Terme, Italy, June 6-11, 2010 PART B including: Symposium PDF

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Extra info for 12th INTERNATIONAL CERAMICS CONGRESS Proceedings of the 12 th International Ceramics Congress, part of CIMTEC 2010- 12 th International Ceramics Congress and 5th Forum on New Materials Montecatini Terme, Italy, June 6-11, 2010 PART B including: Symposium

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A two-step acid-base catalyzed synthesis is used, being the obtained gels dried at atmospheric pressure, in the case of xerogels, and in supercritical conditions, for aerogels. Density and thermal conductivity must be made as low as possible for the sought application and only highly porous materials can fulfill this requirement. The obtained xerogels and aerogels, either with MTMS or MTES, show very promising properties for thermal insulation in Space, when methanol is used as solvent. The more suitable materials are obtained with MTMS and exhibit very low density (80-100 kg/m3), very high surface area (~ 400 m2/g) and small pore size (~ 30-40 Å).

M − OH + OH − M − → − M − O − M − + H 2 O . (6) − M − OH + RO − M − → − M − O − M − + ROH . (7) The as synthesized aluminum-containing film, once pyrolysed, forms amorphous alumina. The pyrolysys is performed under a 1 bar argon atmosphere. The temperature is risen to 900°C and held for 4 hours. Then the samples are heat treated for 1 hour under a static 1 bar pressure, either at 26 12th INTERNATIONAL CERAMICS CONGRESS PART B 1200°C under an argon atmosphere to form α-Al2O3 or from 1200°C to 1600°C under a nitrogen atmosphere to form aluminum nitride.

Z. Zhang, Chem. , 14 (2002) 3808. [17] W. Choi, A. R. Hoffmann, J. Phys. , 98 (1994) 13669. [18] Y. Aita, M. Komatsu S. Yin, and T. Sato, J. , 177 (2004) 3235 [19] S. Yin, Y. Aita, M. Komatsu, J. Wang, Q. Tang, and T. Sato, J. Mater. , 15 (2005) 674 [20] P. Zhang, B. Liu, S. Yin, Y. Wang, V. Petrykin, M. Kakihana, and T. Sato, Mater. Chem. , 116 (2009) 269 [21] S. Yin, H. Hasegawa, D. Maeda, M. Ishitsuka, T. Sato, J. Photochem. Photobiol. , 163 (2004) 1 [22] M. 41 Tailored Silica Based Xerogels and Aerogels for Insulation in Space Environments Luisa Durães1, a, Marta Ochoa1,b, António Portugal1,c, Nelson Duarte2,d, João Paulo Dias2,e, Nuno Rocha3,f and Jessica Hernandez3,g 1 Department of Chemical Engineering, Univ.

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12th INTERNATIONAL CERAMICS CONGRESS Proceedings of the 12 th International Ceramics Congress, part of CIMTEC 2010- 12 th International Ceramics Congress and 5th Forum on New Materials Montecatini Terme, Italy, June 6-11, 2010 PART B including: Symposium by Edited by Pietro VINCENZINI World Academy of Ceramics and National Research Council, Italy Co-edited by Ralf RIEDEL Technical University of Darmstadt, Germany Alexander G. MERZHANOV ISMAN, Russia Chang-Chun


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